Complete kit for free and total SO2 determination (Ripper method), with an automatic self-zeroing burette

Manual titration of sulphurous anhydride

This kit includes a 25ml automatic self-zeroing burette on amber glass flask, with rubber bulb and siphon, a stand, pipettes, an Erlenmeyer flask and the reagents and titrated solutions.

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  • 119901- Complete kit for SO2 determination with auto-zeroing burette
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  • 119901-Complete kit for SO2 determination with auto-zeroing burette

PRINCIPLE

The free sulphurous anhydride is titrated directly in the sample with a titrated iodine solution in the presence of a starch indicator. Subsequently and on a second sample, the SO2 is set free of the combinations it forms with an alkaline solution. Then, the same titration as above is done again and the total SO2 is obtained. The difference between the 2 results gives the combined SO2.

EQUIPMENT AND REAGENTS

  • Stand, rod, and clamp for burette
  • 1 Automatic self-zeroing burette (25 ml) (Ref. 600148)
  • 1 Rubber bulb for automatic burette (Ref. 606000)
  • 1 Siphon for ground-joint flask (Ref. 600194)
  • Green clip for ground-joint assembly (Ref. 600195)
  • 1 VERSILIC hose (diameter 5/7) (Ref. 617602)
  • 1 Amber glass ground-joint flask (500ml) (Ref. 600193)
  • 1 Grey-blue stopper N°10 (Ref. 650110P)
  • 1 Erlenmeyer graduated ground-joint flask (250 ml) (Ref. 615250E)
  • 1 2-mark volumetric pipette (50 ml) (Ref. 603010)
  • 1 2-mark volumetric pipette (25 ml) (Ref. 603025)
  • 1 2-mark volumetric pipette (10 ml) (Ref. 603050)
  • 1 Dropping-pipette with rubber bulb (Ref. 630000)
     
  • 500 ml of iodine solution N/50 (Ref. 936500)
  • 500 ml of sodium hydroxide 1 – 125N (Ref. 934500)
  • 500 ml of diluted sulphurous acid 1/10 (932500)
  • 125 ml of indicator solution (Ref. 937125)
 

WARNING

The sulphurous anhydride is a dissolved gas, which constantly escapes from liquid. To minimize this loss, it is important to:
 
- Carefully take the sample, cork it immediately, and keep it at a cool place after analysis. 
- Prepare the material and the products before uncorking the sample.
- Quickly measure the sample and proceed immediately to titration. 
 

Produits associés

Sulphuric acid in 1/10 - 500 ml

932500Sulphuric acid in 1/10 - 500 ml

Soda 1,125N - 500 ml

934500Soda 1,125N - 500 ml

Iodine N/50 - 500 ml

936500Iodine N/50 - 500 ml

Starch - 125 ml

937125Starch - 125 ml

119901